Optimasi Metode Ekstraksi dengan Wet Peroxide Oxidation (WPO) Untuk Identifikasi Mikroplastik Jenis Polyamide (PA)

Authors

  • Pramadhani Pramadhani Program Studi Kimia, Universitas Negeri Padang, Indonesia
  • Indang Dewata Program Studi Kimia, Universitas Negeri Padang, Indonesia

DOI:

https://doi.org/10.31004/jptam.v7i3.10228

Keywords:

Mikroplastik, Poliamida, Nilon 6,6, Ekstrasi, Wet Peroxide Oxidation (WPO), Katalis Fe(II), Hidrogen Peroxida

Abstract

Penelitian ini bertujuan untuk menentukan kondisi optimum dari suatu metode identifikasi mikroplastik yaitu metode ekstraksi dengan WPO. Pada penelitian ini sampel yang digunakan adalah poliamida berupa nilon 6,6 yang dibuat menjadi ukuran mikroplastik lalu di lakukan proses perendaman selama lebih dari sebulan dengan membiarkan pengotor organik menutupinya agar menyamakan dengan kondisi di lingkungan. Penentuan Kondisi optimum WPO yaitu Variasi Suhu pengovenan (70 oC, 80 oC, 90oC, 100oC dan 110 oC), Variasi Konsentrasi Katalis Fe(II) (0,025 M,0,05 M,0,075 M,0,1 M, dan 0,125 M) dan Variasi Suhu pemanasan reaksi WPO (30oC, 45oC, 60oC, 75oC, dan 90oC). Pada Hasil Penelitian diperoleh Kondisi Optimum Suhu Pengovenan yaitu 90 oC dengan menghasilkan massa mikroplastik sebanyak 0,8989 gr,dan 0,1 M untuk katalis Fe(II) 1.1045 gr,dan suhu pemanasan 75 oC sebanyak 1,5473 gr. Karakterisasi menggunakan mikroskop mendapati bentuk serat poliamida nilon adalah fiber dan karakterisasi FTIR mendapati adanya puncak N-H yang berintensitas tinggi pada sampel rendaman,Serta banyaknya Pengotor-pengotor lainnya sesuai hasil XRF yang sudah dihilangkan pada sampel kondisi optimum yang sudah bersih dari pengotor-pengotornya.

References

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Published

22-10-2023

How to Cite

Pramadhani, P., & Dewata, I. (2023). Optimasi Metode Ekstraksi dengan Wet Peroxide Oxidation (WPO) Untuk Identifikasi Mikroplastik Jenis Polyamide (PA) . Jurnal Pendidikan Tambusai, 7(3), 22907–22915. https://doi.org/10.31004/jptam.v7i3.10228

Issue

Vol. 7 No. 3 (2023): Desember 2023

Section

Articles of Research

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